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Helpful answers
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Sep 17, 2012 9:46 AM in response to Pagalby planb77,The next time the iPod is frozen on the Do Not Disconnect screen, try resetting it by pressing and holding both the Select/Center and Menu buttons together long enough for the Apple logo to appear.
Otherwise, make sure you are always properly ejecting the device from your Mac to prevent this from happening.
As for your iPod not being recognized in iTunes, have you worked through all of the suggestions here?
iPod not recognized in iTunes and Mac desktop
B-rock