Deleted 200 GB file from an APFS volume but space not released
I am runnng Mojave 10.14.6 on an iMac. My APFS container disk has 5 volumes. I boot from the 2nd volume in case that matters. The first volume, Data, is not backed up by Time Machine and that is where I deleted the 200 GB file. I also emptied the trash.
Just to confirm that Time Machine is not the problem, I did run
sudo tmutil thinLocalSnapshots / 10000000000 4
It deleted 5 local snapshots but this did not free up any disk space on volume Data. This is the solution to this problem listed on other threads.
I back up volume Data using SuperDuper but I need to free up this space because my back-up drive is not otherwise large enough. Can anyone help?
iMac 27" 5K, macOS 10.14